本书根据中国药科大学高质量发展、“双一流”建设和化学基础课程教学改革的需要编写而成，侧重药学研究领域仪器分析实验技能和科研思维的培养，同时关注了仪器分析实验新技术，力求培养学生的实验动手能力和分析问题、解决问题的能力。

本书分为6章，包括仪器分析实验基础知识、电化学分析、光谱分析、色谱分析、色谱-质谱联用法及设计类实验，共45个实验，以及6个设计实验选题。内容采用中英文对照，便于双语教学。

本书可作为高等学校药学类专业本科生仪器分析实验课程教材，也可供医学、食品及化学化工等相关学科实验教学和分析工作者的参考用书。

前辅文
Chapter 1 Basic Knowledge of Instrumental Analysis Experiment
  1.1 General Knowledge of Laboratory Safety
  1.2 Experimental Report
  1.3 Disposal of Chemical Laboratory Waste
  1.4 Colored Cylinder Mark for Gases and the Precautions of Gas Cylinders for Use in Laboratory
  1.5 Data Processing Software Commonly Used in Instrumental Analysis Experiments: Introduction to Origin 2018 Software
Chapter 2 Electrochemical Analysis
  Experiment 2.1 Determination of pH Values of Liquid Pharmaceutical Preparations
  Experiment 2.2 Potentiometric Titration Analysis of Phosphoric Acid and Determination of Dissociation Constant
  Experiment 2.3 Determination of Procaine Hydrochlorid by Dead-Stop Titration
  Experiment 2.4 Determination of Caffeine by Potentiometric Titration
  Experiment 2.5 Determination of Fluoride Ion in Drinking Water by Fluoride Ion Selective Electrode
  Experiment 2.6 Determination of Water Content in Antibiotic Drugs
Chapter 3 Spectral Analysis
  Experiment 3.1 Solvent Effect of Ultraviolet Absorption Spectra of Organic Compounds
  Experiment 3.2 Determination of the Absorption Coefficient of API
  Experiment 3.3 Identification and Determination of Vitamin B, Injection by Ultraviolet-visible Spectrophotometry
  Experiment 3.4 Condition Optimization for Colorimetric Determination of Iron with 1, 10-Phenanthroline
  Experiment 3.5 Colorimetric Determination of Trace Iron in Water with 1, 10-Phenanthroline
  Experiment 3.6 Determination of Sulfamethoxazol in the Compound Sulfamethoxazole Tablets by the Dual-Wavelength Method
  Experiment 3.7 Determination of Adrenalone in Adrenaline by Ultraviolet-visible Spectrophotometry
  Experiment 3.8 Preparation and Spectral Determination of Samples with Different States in Infrared Spectrophotometry
  Experiment 3.9 Determination of the Drug Chemical Structure by Infrared Spectrophotometry
  Experiment 3.10 Determination of Magnesium in Tap Water by Atomic Absorption Spectrophotometry
  Experiment 3.11 Determination of Calcium in Calcium Gluconate Oral Solution by Atomic Absorption Spectrometry
  Experiment 3.12 Determination of Cadmium and Lead in Salvia miltiorrhiza by Inductively Coupled Plasma-Atomic Emission Spectrometry
  Experiment 3.13 Determination of Heavy Metals in Soil by Inductively Coupled Plasma-Atomic Emission Spectrometry
  Experiment 3.14 Excitation and Emission Spectra of Anthracene by Fluorescence Spectroscopy
  Experiment 3.15 Determination of Acetylsalicylic Acid and Salicylic Acid in Aspirin Tablets by Fluorescence Analysis
  Experiment 3.16 Determination of Aluminum Ion in Water by Fluorescence Analysis
  Experiment 3.17 Assay of Reserpine Tablets by Fluorescence Analysis
  Experiment 3.18 Determination of Quinine in Tonic Water by Standard Addition Method
  Experiment 3.19 Structure Elucidation of Aspirin by 'H Nuclear Magnetic Resonance Spectroscopy
Chapter 4 Chromatographic Analysis
  Experiment 4.1 Activity Determination of Silica Gel Adhesive Thin Layer
  Experiment 4.2 Identification of Buguzhi (Fructus Psoraleae) by Thin Layer Chromatography
  Experiment 4.3 Separation and Identification of Methionine and Glycine by Paper Chromatography
  Experiment 4.4 Determination of Dead Time and Content of Alkane Mixture with Normalization Method by Gas Chromatography
  Experiment 4.5 Effect of Mobile Phase Velocity on Column Efficiency in Gas Chromatography
  Experiment 4.6 Determination of Alcohol in Tincture by Gas Chromatography
  Experiment 4.7 Determination of Residual Solvent by Temperature Programmed Capillary Gas Chromatography
  Experiment 4.8 Evaluation of the High Performance Liquid Chromatography Performance and Calculation of the Chromatographic Parameters
  Experiment 4.9 Determination of Salicylic Acid Impurity in Aspirin by High Performance Liquid Chromatography
  Experiment 4.10 Determination of Caffeine in Food by High Performance Liquid Chromatography
  Experiment 4.11 Determination of Nandrolone Phenylpropionate by High Performance Liquid Chromatography
  Experiment 4.12 Determination of Sulfamethoxazole and Trimethoprim in Compound Sulfamethoxazole Tablet by Capillary Electrophoresis
  Experiment 4.13 Separation of Chiral Drug Enantiomer by Capillary Zonc Electrophoresis
Chapter 5 Chromatography-Mass Spectrometry
  Experiment 5.1 Performance Verification of Gas Chromatography-Mass Spectrometer
  Experiment 5.2 Performance Verification of High Performance Liquid Chromatography-Mass Spectrometer
  Experiment 5.3 Determination of Eugenol in Caryophylli Flos by Gas Chromatography-Mass Spectrometr
  Experiment 5.4 Determination of p-Phenylenediamine in Hair Dyes by Gas Chromatography-Mass Spectrometry
  Experiment 5.5 Determination of Paracetamol by Liquid Chromatography-Mass Spectrometry
  Experiment 5.6 Determination of Sulfonamides by Liquid Chromatography-Mass Spectrometry
  Experiment 5.7 Determination of Isosorbide-5-Mononitrate in Human Plasma by Ultra-high Performance Liquid Chromatography-Mass Spectrometry
Chapter 6 Designing Experiment
  6.1 Overview
  6.2 General Steps of Designing for the Analysis Scheme
  6.3 Analysis of Scheme Design Cases
  6.4 Typical Example of Designing Experiment
  6.5 Reference Topics of Designing Experiment
Reference
Appendix